Enviar artigo por via de e-mail Reaction of N-sulfinyltrifluoromethanesulfonamide with succinyl chloride
- Autores: Tolstikova L.L1, Sterkhova I.V1, Shainyan B.A1
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Afiliações:
- A.E. Favorsky Irkutsk Institute of Chemistry, Siberian Branch, Russian Academy of Sciences
- Edição: Volume 59, Nº 3 (2023)
- Páginas: 411-414
- Seção: Articles
- URL: https://modernonco.orscience.ru/0514-7492/article/view/666377
- DOI: https://doi.org/10.31857/S0514749223030138
- EDN: https://elibrary.ru/TQOSNR
- ID: 666377
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Resumo
N -Sulfinyltrifluoromethanesulfonamide reacts with succinyl chloride to form 1-[(trifluoromethyl)sulfonyl]pyrrolidine-2,5-dione in high yield. The structure of the product was proved by X-ray diffraction analysis. The product is opened with ethanol under mild conditions selectively at the C-N bond to form (1 E )-4-ethoxy-4oxo- N -[(trifluoromethyl)sulfonyl]butanimidic acid.
Sobre autores
L. Tolstikova
A.E. Favorsky Irkutsk Institute of Chemistry, Siberian Branch, Russian Academy of Sciences
Email: tolstikova@irioch.irk.ru
I. Sterkhova
A.E. Favorsky Irkutsk Institute of Chemistry, Siberian Branch, Russian Academy of Sciences
Email: tolstikova@irioch.irk.ru
B. Shainyan
A.E. Favorsky Irkutsk Institute of Chemistry, Siberian Branch, Russian Academy of Sciences
Email: tolstikova@irioch.irk.ru
Bibliografia
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- Толстикова Л.Л., Шаинян Б.А., Стерхова И.В., Беловежец Л.А. ЖОрХ. 2020, 56, 83-87.
- Tolstikova L.L., Shainyan B.A., Sterkhova I.V., Belovezhets L.A. Russ. J. Org. Chem. 2020, 56, 63-67. doi: 10.1134/S107042802001011X
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